We have successfully
designed and constructed the evaporator systems to improve the vital evaporation and distillation stages for
our clients' Biodiesel facilities.
We have successfully provided optimization of existing
systems as well as providing new separation systems for
biodiesel companies on
continents around the
World. We also trouble shoot existing biodiesel
installations to improve their performance.
TYPICAL BIODIESEL
EVAPORATIVE SEPARATION PROCESS STEPS
Biodiesel (methyl
ester) is manufactured through the trans-esterification of a
variety of vegetable oils either virgin or used/reclaimed by
using methanol and KOH/ NaOH as catalysts. Methanol is
present in excess. The reaction and process are either
batch or continuous but traditionally batch.
There are several
separations which are necessary in the Biodiesel process:
- Biodiesel
/methanol separation
- Glycerin
/methanol separation
- Biodiesel
/water separation
- methanol /
water separation
Optional: 99.5% wt
Glycerin can be achieved by using a vacuum distillation
column.
TYPICAL VOBIS
BIODIESEL SEPARATION PROCESS STAGE DESCRIPTIONS
Following the
reaction stage our systems are implemented to provide the
following separations.
1.
Evaporator for biodiesel /methanol separation
Feed: 93% biodiesel and 7% w/w methanol
Bottoms stream will contain less than
5,000 ppm (0.5%) methanol
Operation: Continuous, 24/7
Operating pressure: Atmospheric
2.
Evaporator for glycerin /methanol separation
Feed: 58% glycerin and 42 % w/w methanol
Bottoms stream will contain less than
5,000 ppm (0.5%) methanol
Operation: Continuous, 24/7
Operating pressure: Atmospheric.
3.
Evaporator for biodiesel /water separation
After the washes they have 1% to 3% water
which must be evaporated.
Feed: 98% biodiesel and 2 % w/w water
Bottoms stream will contain less than
5,000 ppm (0.5%) water
Operation: Continuous, 24/7
Operating pressure: Atmospheric.
4.
Methanol / water separation.
Feed: Feed to column is 95% methanol and
5% water (could be 98% vs. 2%)
Methanol output stream 99.9% methanol
Bottoms stream will contain 5% water
Operation: Continuous, 24/7
Operating pressure: Atmospheric.
Optional: 99.5% wt
Glycerin can be achieved by using our vacuum distillation
column design.
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